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To confirm the influence of MoO3 coating, we analyzed the cycled electrodes. The FE-SEM and HRTEM images of the pristine LNMO and LNMO-MoO3-2 electrode materials were obtained after 500 cycles at different rates between 1 and 10 C (Figure S5). The results revealed that the MoO3 coating layer effectively protected the LNMO cathode from HF attacks, whereas cracks in the surface were observed on the pristine electrode because of the side reaction between LNMO and electrolyte species. In addition, we examined the pristine LNMO and LNMO-MoO3 cathode after cycling testing with XRD analysis. As observed in Figure S6, the LNMO-MoO3 cathode had a much sharper lower angle change than the pristine LNMO. The MoO3 coating layer effectively protects the LNMO from electrolyte species (HF) and stabilizes the crystal structure of the LNMO during the high voltage operation. From the results, we confirmed that the MoO3 layer has a significant effect on controlling the dissolution of Mn and Ni in LNMO. Therefore, the MoO3 coating layer exhibited the best protection performance of the LNMO cathode materials at high-voltage operation of the battery system. Finally, we compared and summarized the rate capability and cycling performance of the MoO3-coated LNMO cathode material with other reported coating materials [20,22,23,39,40,41,42,43,44,45,46,47,48,49,50]. The comparison results can be seen in Table 1. Recently, Bai et al. [50] reported the effect of MoO3 coating on the LNMO spinel cathode by mixing the MoO3 powder with the LNMO cathode with the annealing process. Their report results show that the 2 wt.% MoO3 coated-LNMO is worse than our LNMO-MoO3-2 cathode. Our LNMO-MoO3-2 cathode showed excellent discharge capacity at high rates from 1 to 10 C. Furthermore, the resulting capacity retention at 10 C was considerably stable throughout the 500 cycles. Moreover, electrolyte decomposition is a concern during high-voltage operation. In this case, single oxides are a promising candidate for protective coating and can be extensively used in high-voltage LIBs. 2ff7e9595c
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